UEM - Mass spectrometry unit

GINYS-ICRA-002
The Mass Spectrometry Unit (MSU) aims to be a benchmark in the determination of emerging chemical pollutants in wastewater, natural water and drinking water.
By using technologically advanced instrumentation it offers analytical solutions for the identification and quantification of worldwide relevant organic contaminants at trace levels.
The MSU splits in two subunits according to the chromatographic technique coupled to mass spectrometry:

1) The Gas Chromatography Mass Spectrometry Unit (UEM GCMS) focuses its activity on the identification and quantification of organic compounds belonging to different families, such as polycyclic aromatic hydrocarbons, disinfection by-products, etc., through multiresidue methodologies.
The availability of state-of-the-art equipment allows to face the challenges that arise in environmental topics, both from the point of view of sensitivity and monitoring of new emerging pollutants.

2) The Liquid Chromatography Mass Spectrometry Unit (UEM LCMS) is highly specialized in target analysis of organic contaminants in aqueous samples using multiresidue analytical methods. Our catalogue includes more than 150 compounds such as drugs, antibiotics, pesticides, endocrine disruptors, etc.
It also offers a new service for non-target analysis throughout Liquid Chromatography coupled to High Resolution Mass Spectrometry (LC-HRMS).

Services

Gas Chromatography Coupled to Mass Spectrometry (GC-MS)
0.- Service for weighing of toxic/cytotoxic compounds in a safety cabin.
1.- Volatile Fatty Acids
2.- Methane
3.- Disinfection By-products (DBPs)
4.- Volatile Organic Compounds (VOCs)
5.- Polycyclic Aromatic Hydrocarbons (PAHs)
6.- Organochlorine Pesticides (POCs)
7.- Triclosan and metabolites
8.- Nitrosamines
9.- Haloacetic acids, under preparation
10.- Determination of microplastics, under preparation
11.- Di(2-ethylhexyl) phthalate (DEHP)

Liquid Chromatography Coupled to Mass Spectrometry (LC-MS)
1.- Pesticides
2.- Antibiotics
3.- Endocrine Disruptors (EDCs)
4.- Watch List
5.- Pharmaceuticals (PhACs)
6.- Non-directed analysis

Equipment

  • Gas Chromatograph coupled a triple quadrupole Mass Spectrometer system (GC-MS/MS), TRACE 1300 TSQ9000, Thermo Fisher Scientific.
  • Gas Chromatograph (GC) with Flame Ionization Detector (FID) and Electron Capture Detector (ECD), Trace GC Ultra, Thermo Fisher Scientific.
  • Pyrolyzer coupled to a Gas Chromatograph with a single quadrupole Mass Spectrometry (Pyr-GC/MS), Pyr EGA/PY-3030D, Frontier, GC 8890 MS5977B Inert Plus, Agilent.
  • Ultra-Performance Liquid Chromatography triple Quadrupole Mass spectrometry (UPLC-MS) hydrid Linear Ion Trap (LIT), Acquity UPLC-MS QTRAP 5500, Waters-SCIEX.
  • Ultra-Performance Liquid Chromatography triple Quadrupole Mass spectrometry (UPLC-MS), EQUAN UPLC-MS TSQ Vantage, Thermo Fisher Scientific.
  • Ultra-Performance Liquid Chromatography High Resolution Mass Spectrometry (UPLC-HRMS), Vanquish UPLC-HRMS Orbitrap Exploris 120, Thermo Fisher Scientific.

Staff

Cap d'Unitat
Sara Insa | sinsa@icra.cat | (+34) 608 51 02 53 | ORCID | PRC Page
Diana Álvarez Muñoz | dalvarez@icra.cat | (+34) 689 26 24 64 | ORCID
Tècnic Unitat
Andrea Peris Domes | aperis@icra.cat | (+34) 972 18 33 80 | ORCID
Marta López Martínez | mlopez@icra.cat | (+34) 972 18 33 80 | ORCID
Adrià Robles Briones | arobles@icra.cat | (+34) 972 18 33 80 | ORCID

INSTITUTE

ICRA - Institut Català de Recerca de l'Aigua

Parc Científic i Tecnològic de la UdG
Edifici H2O
Emili Grahit, 101

17003 Girona http://www.icra.cat/

DOMAINS RIS3CAT

  • Food system
  • Sistema d'energia i recursos
  • Education and knowledge generation system
  • Industrial system
  • Socio-sanitary system

CATEGORIES

  • TECHNOLOGICAL EQUIPMENT
    • Other specializated laboratories
    • Spectrometry, chromatography and spectroscopy

RATES AND ACCESS

Availability Level: Low
Access Procedures:
Contact to the responsible for the MSU:
GC/MS
: Sara Insa (sinsa@icra.cat)
LC/MS
: Diana Álvarez (dalvarez@icra.cat)
CERCA - Ginys